They look like a form of spherulites, which don't diffract as is but can likely 
be optimized by matrix optimization, seeding, and such methods. Or in fact they 
might just be crystals that need to be optimized into diffracting crystals. 
Check this link for some ideas:

https://xray.teresebergfors.com/tutorial-3/

Good luck!


________________________________
From: CCP4 bulletin board <CCP4BB@JISCMAIL.AC.UK> on behalf of 
careinaedgo...@yahoo.com <000002531c126adf-dmarc-requ...@jiscmail.ac.uk>
Sent: Wednesday, November 8, 2023 10:00 AM
To: CCP4BB@JISCMAIL.AC.UK <CCP4BB@JISCMAIL.AC.UK>
Subject: [ccp4bb] What could these crystals be?

Hi all
We have been trying with no success to crystalize a protein. Recently we got 
these strange shape "crystals". They are hard and flat but they do not diffract 
at all. Any ideas as to what could cause this?
Careina

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