I was afraid of that. Unfortunately, my sample is a powder containing about
3 or 4 different alkali phosphates, so a little tricky.

On Tue, 24 Dec 2024, 15:51 Alan W Hewat, <alan.he...@neutronoptics.com>
wrote:

> Current (2023) knowledge, including main x-ray lines, is summarised on
> https://www.mindat.org/min-2712.html
> which also links to the extensive American Mineralogy database (which does
> not include Millisite). If you have a clean sample, you may need neutrons
> to distinguish it from similar hydrated minerals, but it's not obvious that
> it's interesting enough :-)
> Alan
> ________________________________
> Dr Alan Hewat, NeutronOptics
> Grenoble, FRANCE (from phone)
> alan.he...@neutronoptics.com
> +33.476984168 VAT:FR79499450856
> http://NeutronOptics.com/hewat
> _______________________________
>
>
> On Tue, 24 Dec 2024, 04:49 Matthew Rowles, <rowle...@gmail.com> wrote:
>
>> Hi all
>>
>> Does anyone know of a published crystal structure for millisite?
>>
>> It is nominally (Na,K)CaAl6(PO4)4(OH)9·3H2O
>> Tetragonal, a=7, c=19.07 Å
>> See http://www.minsocam.org/ammin/AM45/AM45_547.pdf
>>
>>
>> or maybe anything possibly isostructural/morphous? It's pretty close to
>> wardite, but has an extra hydroxide and water.
>>
>> ICDD PDF4+ has nothing, Various searches on COD haven't revealed
>> anything. I don't have access to ICSD.
>>
>> Thanks
>>
>>
>> Matthew Rowles
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