Current (2023) knowledge, including main x-ray lines, is summarised on
https://www.mindat.org/min-2712.html
which also links to the extensive American Mineralogy database (which does
not include Millisite). If you have a clean sample, you may need neutrons
to distinguish it from similar hydrated minerals, but it's not obvious that
it's interesting enough :-)
Alan
________________________________
Dr Alan Hewat, NeutronOptics
Grenoble, FRANCE (from phone)
alan.he...@neutronoptics.com
+33.476984168 VAT:FR79499450856
http://NeutronOptics.com/hewat
_______________________________


On Tue, 24 Dec 2024, 04:49 Matthew Rowles, <rowle...@gmail.com> wrote:

> Hi all
>
> Does anyone know of a published crystal structure for millisite?
>
> It is nominally (Na,K)CaAl6(PO4)4(OH)9·3H2O
> Tetragonal, a=7, c=19.07 Å
> See http://www.minsocam.org/ammin/AM45/AM45_547.pdf
>
>
> or maybe anything possibly isostructural/morphous? It's pretty close to
> wardite, but has an extra hydroxide and water.
>
> ICDD PDF4+ has nothing, Various searches on COD haven't revealed anything.
> I don't have access to ICSD.
>
> Thanks
>
>
> Matthew Rowles
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