Topas can model them quite well. The functionality was introduced in
version 5.

On Mon, 4 Sep 2023, 00:54 Kurt Leinenweber, <ku...@asu.edu> wrote:

> Hi,  Are these things modeled in Rietveld programs, by chance?  It seems
> like a lot of baggage to put in a refinement but if it makes the results
> better…
>
>
>
>    - Kurt
>
>
>
> *From:* rietveld_l-requ...@ill.fr <rietveld_l-requ...@ill.fr> *On Behalf
> Of *Thomas Gegan
> *Sent:* Sunday, September 3, 2023 9:16 AM
> *To:* Bish, David L <b...@indiana.edu>; Shay Tirosh <stiro...@gmail.com>;
> Fernando Igoa <fer.igoa.1...@gmail.com>
> *Cc:* Rietveld List (rietveld_l@ill.fr) <rietveld_l@ill.fr>
> *Subject:* RE: [EXT] Re: [External] Re: Step-like basline
>
>
>
> I agree with a Ni absorption edge, possibly with a Kβ peak around 38° 2θ.
>
>
>
> *Tom Gegan*
> Chemist III
>
>
>
> Phone: +1 732 205-5111, Email: tom.ge...@basf.com
> Postal Address: BASF Corporation, , 25 Middlesex Essex Turnpike, 08830
> Iselin, United States
>
>
>
> *From:* rietveld_l-requ...@ill.fr <rietveld_l-requ...@ill.fr> *On Behalf
> Of *Bish, David L
> *Sent:* Sunday, September 3, 2023 7:08 AM
> *To:* Shay Tirosh <stiro...@gmail.com>; Fernando Igoa <
> fer.igoa.1...@gmail.com>
> *Cc:* Rietveld List (rietveld_l@ill.fr) <rietveld_l@ill.fr>
> *Subject:* [EXT] Re: [External] Re: Step-like basline
>
>
>
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>
> Hello Shay,
>
> I think it is probably related to "tube tails". You can read about this in
> the literature (e.g., on the BGMN web site) and you can model it in some
> Rietveld software such as Topas. You don't normally notice this but it
> becomes apparent with higher-intensity peaks.
>
>
>
> Regards,
>
> Dave
> ------------------------------
>
> *From:* rietveld_l-requ...@ill.fr <rietveld_l-requ...@ill.fr> on behalf
> of Fernando Igoa <fer.igoa.1...@gmail.com>
> *Sent:* Sunday, September 3, 2023 3:06 AM
> *To:* Shay Tirosh <stiro...@gmail.com>
> *Cc:* Rietveld List (rietveld_l@ill.fr) <rietveld_l@ill.fr>
> *Subject:* [External] Re: Step-like basline
>
>
>
> This message was sent from a non-IU address. Please exercise caution when
> clicking links or opening attachments from external sources.
>
>
>
> Hey Shay,
>
>
>
> Are you using a motorized slit during the measurement? These may open up
> abruptly to compensate for the angular dependence of the footprint and thus
> generate an abrupt increase in the intensity.
>
>
>
> Hope it helps :)
>
>
>
> On Sun, Sep 3, 2023, 8:50 AM Shay Tirosh <stiro...@gmail.com> wrote:
>
> Dear Rietvelders
>
> I am attaching a zoom-in on a diffraction profile.
>
> My question is what is the origin of the step-like profile next to a very
> large reflection peak?
>
> Is it a sample preparation problem?
>
> Is it part of the baseline?
>
> Thanks
>
> Shay
>
> --
>
>
>
>
>
>
>
>
>
>
>
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