Hey Shay, Are you using a motorized slit during the measurement? These may open up abruptly to compensate for the angular dependence of the footprint and thus generate an abrupt increase in the intensity.
Hope it helps :) On Sun, Sep 3, 2023, 8:50 AM Shay Tirosh <[email protected]> wrote: > Dear Rietvelders > I am attaching a zoom-in on a diffraction profile. > My question is what is the origin of the step-like profile next to a very > large reflection peak? > Is it a sample preparation problem? > Is it part of the baseline? > [image: image.png] > Thanks > Shay > -- > > > > > > > > > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > Please do NOT attach files to the whole list <[email protected] > > > Send commands to <[email protected]> eg: HELP as the subject with no body > text > The Rietveld_L list archive is on > http://www.mail-archive.com/[email protected]/ > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > >
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <[email protected]> Send commands to <[email protected]> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/[email protected]/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
