Dear Breogán,
most probably, you have to make alignment of the primary beam cut. If
you use focusing mirror, the beam cutter should be there, see the
picture here:
https://drive.google.com/file/d/1SLbYfw90cikML_tE19Xp0ZHgBBNtTc9Y/view?usp=sharing
Jan
Dne 2019-06-11 11:17, Cristóbal Verdugo napsal:
Hi Breogan,
Not with Panalytical but with Bruker diffractometer I had the same
problem, we are close to the direct beam. What I did was to cronstruct
a circular slit to cut the direct beam and now I can measure from 2
degrees.
Please, feel free to contact me for help.
Regards,
Cristóbal
—
Dr. Cristóbal Verdugo-Escamilla
cristobal.verd...@csic.es
Phone. 0034 677350122
El 11 jun 2019 11:10 +0200, Breogán Pato Doldán
<breogan.p...@udc.es>, escribió:
Dear Rietvelders,
First of all, I would like to thank you for your help. I joined the
mailing list during the first year of my PhD studies. The Rietveld
mailing list has proved to be a quite useful tool through these
years.
I have just arrived to a new lab and I am the only one with some
XRPD experience.
Several months ago an Empyrean from Panalytical was installed in the
lab. The diffractometer is configured on transmisión. I have had
some problems recording data at low angles (below 5 degrees) ¿Has
anyone had the same problem?
Best regards,
Breogán Pato
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