Hi Breogan, Not with Panalytical but with Bruker diffractometer I had the same problem, we are close to the direct beam. What I did was to cronstruct a circular slit to cut the direct beam and now I can measure from 2 degrees. Please, feel free to contact me for help.
Regards, Cristóbal — Dr. Cristóbal Verdugo-Escamilla cristobal.verd...@csic.es Phone. 0034 677350122 El 11 jun 2019 11:10 +0200, Breogán Pato Doldán <breogan.p...@udc.es>, escribió: > Dear Rietvelders, > > First of all, I would like to thank you for your help. I joined the mailing > list during the first year of my PhD studies. The Rietveld mailing list has > proved to be a quite useful tool through these years. > > I have just arrived to a new lab and I am the only one with some XRPD > experience. > Several months ago an Empyrean from Panalytical was installed in the lab. The > diffractometer is configured on transmisión. I have had some problems > recording data at low angles (below 5 degrees) ¿Has anyone had the same > problem? > > Best regards, > Breogán Pato > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> > Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text > The Rietveld_L list archive is on > http://www.mail-archive.com/rietveld_l@ill.fr/ > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ >
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
