In 1981 I started as a working student at the Siemens Research Centre in Erlangen, Germany. There was a type F goniometer, equipped with stepping motors installed by local employees. The detector was a Si(Li) enabling switing between CuKa, CuKb and finally even W-radiation with old tubes.

I don't know how long the company was already running this diffractometer, but adding stepping motors was not a commercial solution. Perhaps this was done in cooperation with the research centre in Munich (Germany) where these gonometers were developed.

Later I used this goniometer for my own diploma thesis.

Regards

Robert

At 21:15 31.01.2016, you wrote:
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I think this answers my question.  [By automated I mean simply producing digital data, in x y pairs.]  In 1980, in Bob Snyder’s lab we had an automated Philips; the mounting of the stepper motor was home-brew, but the electronics consisted of out-of-the-box Canberra products.  So I presumed that this not, by any means, the first of the automated lab machines, and was curious as to when first one was commissioned.  Never knew the Type F was sold by Siemens as automated?  What year was this?  Googling “automated siemens type f” yields no joy.
 
Jim
 
 
James P. Cline
Materials Measurement Science Division                 
National Institute of Standards and Technology
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From: alan.he...@gmail.com [ mailto:alan.he...@gmail.com] On Behalf Of Alan Hewat
Sent: Sunday, January 31, 2016 2:27 PM
To: Cline, James Dr. <james.cl...@nist.gov>
Cc: rietveld_l@ill.fr
Subject: Re: Automated XRD Date
 

Neutron diffractometers were automatic well before x-ray diffractometers, and were also first for position sensitive detectors (PSDs) and of course Rietveld refinement. Paper tape control was introduced in the 1950's, computers in the early 1960's and PSD's in the early 1970's. X-rays followed after about 10 years. From memory only. It can't be difficult to Google this.

Alan
On 31 January 2016 at 16:47, Cline, James Dr. <james.cl...@nist.gov> wrote:
Anyone know when/where the first automated powder diffractometer was commissioned?  I’m going to presume it was used with a non-laboratory source

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 Dr. Robert Haberkorn, Universitaet des Saarlandes
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