I guess you are talking about detection limit only, not quantification limit, 
right?
The answer largely depends on your material (scattering power, domain size), 
tube (sampling volume) and counting time. I have seen cases where you can 
clearly see something below 0.1 wt% and cases where already the percent was off 
limits. 
Matteo

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  Matteo Leoni, PhD

  DICAM
  University of Trento
  via Mesiano, 77
  38123 Trento
  Italy

  Tel +39 0461 282416     Fax +39 0461 282672

  e-mail: matteo.le...@unitn.it
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-----Messaggio originale-----
Da: rietveld_l-requ...@ill.fr [mailto:rietveld_l-requ...@ill.fr] Per conto di 
Apu Sarkar
Inviato: giovedì 1 maggio 2014 22.24
A: rietveld_l@ill.fr
Oggetto: Phase volume fraction

Hi,
Can any one tell me what is the minimum phase volume fraction that can be 
detected by a laboratory X-ray diffractometer. In there any reference for this.

I am using the new Empyrean from PANalytical.

Thanks
Apu

Department of Nuclear Engineering
NC State University
Raleigh, USA
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