I guess you are talking about detection limit only, not quantification limit, right? The answer largely depends on your material (scattering power, domain size), tube (sampling volume) and counting time. I have seen cases where you can clearly see something below 0.1 wt% and cases where already the percent was off limits. Matteo
----------------------------------------------------------------- Matteo Leoni, PhD DICAM University of Trento via Mesiano, 77 38123 Trento Italy Tel +39 0461 282416 Fax +39 0461 282672 e-mail: matteo.le...@unitn.it ---------------------------------------------------------------- -----Messaggio originale----- Da: rietveld_l-requ...@ill.fr [mailto:rietveld_l-requ...@ill.fr] Per conto di Apu Sarkar Inviato: giovedì 1 maggio 2014 22.24 A: rietveld_l@ill.fr Oggetto: Phase volume fraction Hi, Can any one tell me what is the minimum phase volume fraction that can be detected by a laboratory X-ray diffractometer. In there any reference for this. I am using the new Empyrean from PANalytical. Thanks Apu Department of Nuclear Engineering NC State University Raleigh, USA
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++