Hi Lachlan,
why not try a STOE-furnace ? The rotating capillary sticks out of the
furnace and thus stays at room temperature.
It works up to about 900°C and I use MoKa1-radiation for (almost) no
absorption. :-D
Cheers, Julius
LACHLAN MACLEAN schrieb:
Hi All
I know this doesn't have direct application to rietveld work (well, I
will be using it), but I am doing time-resolved powder XRD
precipitation experiments in hydrothermal aqueous solutions using 1mm
OD sapphire capillaries, a furnace mounted to our XRD and epoxy. I am
curious whether there are other sealants people have used other than
epoxy, or what type of epoxies people prefer. I'm looking at
temperatures up to 300C.
Thanks for any help
Cheers
Lachlan
- -
Lachlan C.W. MacLean, PhD.
Center for Environmental Kinetics Analysis
413 Deike Building
Pennsylvannia State University
University Park, PA 16801
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