Thank you very much for useful suggestions! :-) Best,
Almu 2014-05-20 9:44 GMT+02:00 Kay Diederichs <kay.diederi...@uni-konstanz.de>: > Dear Almudena, > > if you follow the recommendations given in the "Difficult datasets" > article on XDSwiki, your problem would have a good chance to be solved. > > best wishes, > > Kay > > On Mon, 19 May 2014 18:18:46 +0200, Almudena Ponce Salvatierra < > maps.fa...@gmail.com> wrote: > > >Dear all, > > > >I am looking for some suggestions here. I have lately collected some > >datasets but the spots are very very weak... it is very difficult to > >process them. At times it looks like XDS is stalled or at times it just > >says that it can not interpret the lattice parameters... also while > running > >integrate I have such a message after each range of images: > > > >!!! WARNING !!! REFINEMENT DID NOT CONVERGE > > LAST CORRECTION SHIFT WAS 9.1E-03 (should be < > 1.0E-03) > > > >I guess this is not good at all. And I wonder what to do? Is there any > info > >that I can get out from these data at all? or rather not? > > > >I wonder if the problem is to find the spots, I have tried with HKL2000 > and > >it can't even find enough of them for indexing. > > > >Any ideas are welcome. > > > >Best wishes, > > > >Almudena. > > > >-- > >Almudena Ponce-Salvatierra > >Macromolecular crystallography and Nucleic acid chemistry > >Max Planck Institute for Biophysical Chemistry > >Am Fassberg 11 37077 Göttingen > >Germany > > > > > -- Almudena Ponce-Salvatierra Macromolecular crystallography and Nucleic acid chemistry Max Planck Institute for Biophysical Chemistry Am Fassberg 11 37077 Göttingen Germany
