hlicek
Sent: Wednesday, June 6, 2018 4:56 AM
To: rietveld_l@ill.fr
Subject: getting intensities from multiple powder pattern
Dear all,
I would like to obtain integrated intensities from several (up to 5) powder
patterns that were measured at different temperatures.
My idea is to make fit by Pawl
A second vote for Topas. You can have multiple hkl phases and do a Pawley
refinement. The intensities can be given the same keyword, which forces
them to have the same value. You then refine a scale factor on patterns
2-5, with the 1st one fixed at 1.
Matthew
On 6 June 2018 at 17:02, Norberto Mas
Hi all
I have done it in the past by changing the "refine flag" in the
intensity list of the Pawley refinement with a fake scale factor (one
per dataset - minus the "0th one") multiplying the intensity values of
each reflection.
Just use TOPAS in launch mode.
Norberto
Dear all,
I would like
Dear all,
I would like to obtain integrated intensities from several (up to 5) powder
patterns that were measured at different temperatures.
My idea is to make fit by Pawley (or Le Bail?) method of all datasets at the
same time and keep integrated intensities of individual hkls the same for
al
