A second vote for Topas. You can have multiple hkl phases and do a Pawley refinement. The intensities can be given the same keyword, which forces them to have the same value. You then refine a scale factor on patterns 2-5, with the 1st one fixed at 1.
Matthew On 6 June 2018 at 17:02, Norberto Masciocchi < norberto.mascioc...@uninsubria.it> wrote: > Hi all > I have done it in the past by changing the "refine flag" in the intensity > list of the Pawley refinement with a fake scale factor (one per dataset - > minus the "0th one") multiplying the intensity values of each reflection. > Just use TOPAS in launch mode. > Norberto > > Dear all, > > > > I would like to obtain integrated intensities from several (up to 5) > powder patterns that were measured at different temperatures. > > My idea is to make fit by Pawley (or Le Bail?) method of all datasets at > the same time and keep integrated intensities of individual hkls the same > for all datasets. > > > > Do you know about some software, that can restrain or even fix integrated > intensities between refined datasets? > > > > Thank you in advance, > > Jan > > > > *Ing. Jan Rohlicek, Ph.D.* > > *Institute of Physics CAS* > > * Cukrovarnicka 10/112 162 00 Prague 6* > > *Tel: (+420) 220 318 484* > > *Email: rohli...@fzu.cz <rohli...@fzu.cz>* > > > > > <http://www.avg.com/email-signature?utm_medium=email&utm_source=link&utm_campaign=sig-email&utm_content=emailclient> > Mail > priva di virus. www.avg.com > <http://www.avg.com/email-signature?utm_medium=email&utm_source=link&utm_campaign=sig-email&utm_content=emailclient> > <#m_5331402660391734722_DAB4FAD8-2DD7-40BB-A1B8-4E2AA1F9FDF2> > > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> > <alan.he...@neutronoptics.com> > Send commands to <lists...@ill.fr> <lists...@ill.fr> eg: HELP as the subject > with no body text > The Rietveld_L list archive is on > http://www.mail-archive.com/rietveld_l@ill.fr/ > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > > > > -- > Norberto Masciocchi > Professor of Chemistry > Department of Science and High Technology & To.Sca.Lab. > University of Insubria > Via Valleggio, 11 > 22100 Como - Italy > E-mail: norberto.mascioc...@uninsubria.it > Tel: +39-031-2386613 > Skype: norberto.masciocchi > Website: toscalab.uninsubria.it > Publish in: Chem2 Journal (www.chem2.org)! > > > > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > Please do NOT attach files to the whole list <alan.he...@neutronoptics.com > > > Send commands to <lists...@ill.fr> eg: HELP as the subject with no body > text > The Rietveld_L list archive is on http://www.mail-archive.com/ > rietveld_l@ill.fr/ > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > > >
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
