Re: sealing capillary in a glove box

2023-02-03 Thread miguel gregorkiewitz
Dear Angeles, A couple of minutes ago I sent you the zip file containg the documents of our manipulator to seal capillaries etc. Let me know if you have any.problems! Best Miguel El vie, 3 feb. 2023 15:39, miguel gregorkiewitz escribió: > Dear Angeles, > > Here i send you the zip file contai

Re: sealing capillary in a glove box

2023-02-01 Thread miguel gregorkiewitz
Dear Dharmalingam, A couple of minutes ago I sent you a zip file containg the documents of our manipulator to seal capillaries etc. Let me know if you have any.problems! Best Miguel El jue, 2 feb. 2023 8:30, miguel gregorkiewitz escribió: > Dear Dharmalingam, > > Here i send you a zip file c

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz
Dear Mirela, if you are working with quartz capillaries, i would use Pt for the filament. The plastic parts on the connectors can be removed. I actually did this already in the basic design. Let me know if you can reach the necessary temperature! Best Miguel El mié, 1 feb. 2023 8:18, miguel g

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz
Dear Mirela, A couple of minutes ago I sent you a zip file containg the documents of our manipulator to seal capillaries etc. Let me know if you have any.problems! Best Miguel El mié, 1 feb. 2023 0:22, mirela dragomir escribió: > Dear Miguel, > > I'm also intrigued by your setup and would li

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz
.com_a_stonybrook.edu_pgk_home&d=DwMFaQ&c=aTOVZmpUfPKZuaG9NO7J7Mh6imZbfhL47t9CpZ-pCOw&r=BX8us55AyPAIC_WBilHRkA&m=Ct0KZCwEwpWRcA5CUercOpxFrSByRm-qocG1lq-PEZc&s=joWXazAAemA3JtxXYrqXryS48Uko6JW70pfW7PzQSWc&e=> >>> >>> >>> >>> *From:* riet

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz
&s=joWXazAAemA3JtxXYrqXryS48Uko6JW70pfW7PzQSWc&e=> > > > > *From:* rietveld_l-requ...@ill.fr *On Behalf > Of *miguel gregorkiewitz > *Sent:* Monday, January 30, 2023 7:07 AM > *To:* francois Goutenoire > *Cc:* Rietveld List (rietveld_l@ill.fr) > *Subj

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz
Dear Cristóbal, A couple of minutes ago I sent you a zip file containg the documents of our manipulator to seal capillaries etc. Let me know if you have any.problems! Best Miguel El lun, 30 ene. 2023 14:08, Cristóbal Verdugo escribió: > Dear Miguel, > could you, please, share details about

Re: Sealing capillary in a glove box

2023-01-31 Thread Francois Fauth
Hi Most of MSPD at ALBA users facing this problem (typically battery materials previously filled and sealed in Ar GB) prefer sealing with plastiline (instead of grease) The problem is often sharp cutting the capillary after having filled the capillary  Borosilicate caps appaers more brittle th

Re: Sealing capillary in a glove box

2023-01-30 Thread miguel gregorkiewitz
I constructed an electrical heater which is used with a tunable power supply and a microscope if possible. Let me know if you like to have details of the design! Miguel El lun, 30 ene. 2023 12:01, francois Goutenoire < francois.gouteno...@univ-lemans.fr> escribió: > Dear Rietveld users, > > We

Re: Sealing capillary in a glove box

2023-01-30 Thread Fernando Igoa
Dear François, The easy way we have found to do that is by isolating the open aperture with vacuum grease inside the glove box and theb taking them outside where you can seal them easily with a lighter. Hope it helps Best, Le lun. 30 janv. 2023 à 12:01, francois Goutenoire < francois.gouteno...

RE: Sealing capillary in a glove box

2023-01-30 Thread Radovan Cerny
Dear François, You can just put a bit of vacuum grease, but this is not mechanically very stable. The best is to seal with a drop of fast epoxy glue. Easy to manipulate inside the glove box. Best regards Radovan Radovan Cerny Laboratoire de Cristallographie, DQMP Université de Genève 24, quai