detailed electron density analysis.
Best,
Jon
On 19/06/2015 09:10, Tony Raftery wrote:
Anyone,
Can someone tell me where to source diamond for use as internal standard.
It needs to be ‘ideal’ – small particle size ( 1um would be good),
narrow particle size distribution, elementally pure
one,
>
>
>
> Can someone tell me where to source diamond for use as internal standard.
>
>
>
> It needs to be ‘ideal’ – small particle size ( 1um would be good), narrow
> particle size distribution, elementally pure (which precludes most
> ‘natural’ diamond), fully crystal
Hi Tony
I think we used diamond polishing powder when I was at CSIRO.
Lots of different sizes available.
Matthew
On 19 Jun 2015 3:13 pm, "Tony Raftery" wrote:
> Anyone,
>
>
>
> Can someone tell me where to source diamond for use as internal standard.
>
>
>
Anyone,
Can someone tell me where to source diamond for use as internal standard.
It needs to be 'ideal' - small particle size ( 1um would be good), narrow
particle size distribution, elementally pure (which precludes most 'natural'
diamond), fully crystalline (or near so)
reliable to
> utilize the aluminum peaks (or even the beryllium peaks from my in-situ
> cell window) from my support as an internal standard ?? (even though that
> itself is not in the same plane as my sample)
>
> My initial thoughts would be that I am not able to do so without
&
diffractometer, however my optimization of
the sample alignment has simply been done to maximize my signal to noise ratio.
My question then becomes… is it feasible/reliable to utilize the aluminum peaks
(or even the beryllium peaks from my in-situ cell window) from my support as an
internal standard ?? (even
) 975 5793
FAX (301) 975 5334
-Original Message-
From: rietveld_l-requ...@ill.fr [mailto:rietveld_l-requ...@ill.fr] On Behalf Of
Reinhard Kleeberg
Sent: Thursday, March 26, 2015 7:57 AM
To: rietveld_l@ill.fr
Subject: corundum internal standard alternative?
Dear colleagues,
does anybody know
Dear colleagues,
does anybody know a fine-grained alumina (corundum) material with high
purity, suitable for using as internal standard in quantitative phase
analysis, as an economic alternative for the NIST SRM 676a?
In the past we used American Elements AL-OX-03-S (spray-dried) what
worked
two such uncertainties is much larger than
> the other one it will not make a big effect on the total uncertainty.
>
> I hope this helps or at least generates a useful discusion and
> correction to my proposition if wrong.
>
> Best regards,
> Leo
>
>
> 2013/9/1
diffractometers. Because the in-situ variations also causes sample
displacement, we have been using an added internal standard (Si)
and corrected the 2-theta axis so that the silicon lines are in
correct positions. Because we wanted to be sure that our method is
reproducible, we h
ations also causes sample
> displacement, we have been using an added internal standard (Si) and
> corrected the 2-theta axis so that the silicon lines are in correct
> positions. Because we wanted to be sure that our method is reproducible, we
> have repeated our experiments 5-10 ti
Dear all
I would appreciate some statistical advice. We are measuring cell
parameters variations in-situ of some structures using in-house
diffractometers. Because the in-situ variations also causes sample
displacement, we have been using an added internal standard (Si) and
corrected the 2
Hi all,
This may be a non-issue given the high accuracy of diffraction measurements,
and the internal checks on sample position, such as dependent peaks that lead
to the sample shift, but there is something I've always wondered about when an
internal standard is used in combination
You
should multiply all of the crystalline phases by 5/7 with the remaining 2/7
being your amorphous phases.
-Original Message-From: Ferdinando Costantino
[mailto:[EMAIL PROTECTED]]Sent: Friday, June 15, 2001 9:32
AMTo: [EMAIL PROTECTED]Subject: internal standard for
glass
Dear all
I'm doing quantitative analysis on a mixture
of 6 or 7 phases and I must to know the weight fraction of amorphous
phases.
I'm using Si as internal standard but I'didn't
understand if I must consider the relative or absolute difference between the
real and calc
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