Dear James,
I agree with your chronology of the first full new protein structures by SR
MAD.
The 1975 two wavelength Hoppe and Jakubowksi study of erythrocruorin with Ni
and Co Kalpha Xray tubes is a classic piece of work of in effect MAD phasing .
See the IUCr Anomalous Scattering Conference
On Saturday, 16 March 2013, James Holton wrote:
> The first report of shooting a protein crystal at a synchrotron (I
> think) was in 1976:
> http://www.pnas.org/content/73/1/128.full.pdf
> that was rubredoxin
>
> The first PDB file that contains a "SYNCHROTRON=Y" entry is 1tld
> (trypsin), which
Thank you James, you should write a History book about the modern x-ray times.
Or better make one of those movies you are famous for.
Jürgen
On Mar 16, 2013, at 10:46 AM, James Holton wrote:
The first report of shooting a protein crystal at a synchrotron (I
think) was in 1976:
http://www.pnas.or
The first report of shooting a protein crystal at a synchrotron (I
think) was in 1976:
http://www.pnas.org/content/73/1/128.full.pdf
that was rubredoxin
The first PDB file that contains a "SYNCHROTRON=Y" entry is 1tld
(trypsin), which was deposited in 1989:
http://dx.doi.org/10.1016/0022-2836(
here
http://xdb.lbl.gov/Section2/Sec_2-2.html
Colin
-Original Message-
From: CCP4 bulletin board [mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of DUMAS
Philippe (UDS)
Sent: 13 March 2013 19:22
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Jean Witz (now deceased)
of synchrotron radiation in PX
And indeed this experiment was done properly ... in a suit and tie!
http://www.embl-hamburg.de/aboutus/general_information/HH_about/history/HH-holmes.jpg
A.
PS The journal is indeed a bit obscure ...
On 13 Mar 2013, at 20:22, DUMAS Philippe (UDS) wrote:
> J
Nice account on the subject
J Synchrotron Radiat. 2010 July 1; 17(Pt 4): 433–444.
Published online 2010 May 14. doi: 10.1107/S0909049510011611
Impact of synchrotron radiation on macromolecular crystallography: a personal
view
Zbigniew Dauter,a,* Mariusz Jaskolski,b,* and Alexander Wlodawer,c,*
And indeed this experiment was done properly ... in a suit and tie!
http://www.embl-hamburg.de/aboutus/general_information/HH_about/history/HH-holmes.jpg
A.
PS The journal is indeed a bit obscure ...
On 13 Mar 2013, at 20:22, DUMAS Philippe (UDS) wrote:
> Jean Witz (now deceased) once told
Jean Witz (now deceased) once told me that the following paper is the first
one mentionning data "collection" on a synchrotron.
The journal is not really "obscure" and the paper should easily be found.
The work was done in Germany, if I remember well.
G. Rosenbaum, K.C. Holmes and J. Witz, Synch
> From: CCP4 bulletin board [mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of Harry
> Powell
> Sent: 13 March 2013 15:04
> To: ccp4bb
> Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
>
> Hi
>
> Not sure if this is strictly speaking the first protein *solved* on
Dear Colleagues,
The paper
http://dx.doi.org/10.1107/S0108768185002233
in work led by Howard Einspahr undertaken at SRS 7.2 is a protein structural
specific result from synchrotron radiation.
The MAD method of course yielded totally specific to SR protein crystal
structures. The conceptualisati
mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of
> Harry Powell
> Sent: 13 March 2013 15:04
> To: ccp4bb
> Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
>
> Hi
>
> Not sure if this is strictly speaking the first protein *solved* on a
> synchrotron, but I t
board [mailto:CCP4BB@JISCMAIL.AC.UK] On Behalf Of Harry
Powell
Sent: 13 March 2013 15:04
To: ccp4bb
Subject: Re: [ccp4bb] first use of synchrotron radiation in PX
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of sho
Nothing prescient about that. The MAD concept was first proposed by
Herzberg and Lau in 1967, much before sycnhrotrons were used for protein
crystallography.
Herzenberg, A. & Lau, H. S. M. (1967) Acta. Crystallogr. 22, 24-28.
http://scripts.iucr.org/cgi-bin/paper?S0365110X6740
The PNAS p
Did anyone see this prescient line in the PNAS paper? Seems that the MAD
concept was suggested way back then...
JPK
"While the enhancement of anomalous scattering
has not yet been examined in detail, it is in principle
possible to use data collected at three wavelengths (15) to
completely solve
Hi
Not sure if this is strictly speaking the first protein *solved* on a
synchrotron, but I think this is the first report of shooting protein crystals
at a synchrotron in the widely available literature -
http://www.pnas.org/content/73/1/128.full.pdf+html
Phillips J C, Wloda
Hi all - i'm sure this many will know this : when and what was the first
protein structure solved on a synchrotron?
Thanks in advance
Alan
--
Alan Cheung
Gene Center
Ludwig-Maximilians-University
Feodor-Lynen-Str. 25
81377 Munich
Germany
Phone: +49-89-2180-76845
Fax: +49-89-2180-76999
E-mail
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