Re: NIST-676a
Hi Jim, great news, would be good to have a corundum what can be modelled with an easier profile shape model. Best regards Reinhard Zitat von "Cline, James P. Dr. (Fed)" : Hi all, SRM 676a consisted of Baikowski CR1. This material is of a non-ideal crystallite size distribution: quite broad with tales to large crystallites. SRM 676b was custom made for us by Baikowski with a more uniform crystallite size distribution in the 200 nm region. We are working on the certification, rather complex, see: doi:10.1107/S0108767311014565 . It seems that modern beamlines don't favor the large specimen size needed for our experiments. We have good data from one source, we are looking for some from another as we like to see results from more one machine. Jim James P. Cline Materials Measurement Science Division National Institute of Standards and Technology 100 Bureau Dr. stop 8370 [ B113 / Bldg 217 ] Gaithersburg, MD 20899-8523USA james.cl...@nist.gov https://www.nist.gov/people/james-p-cline (301) 975 5793 -Original Message- From: rietveld_l-requ...@ill.fr On Behalf Of Reinhard Kleeberg Sent: Monday, November 13, 2023 1:51 AM To: rietveld_l@ill.fr Subject: Re: NIST-676a We are using Baikowski CR1 https://www.baikowski.com/en/serie/cr/ Not certified but maybe identical with SRM676a. Scale factors and cell parameters found to be within the errors. Profile shape shows similar features (also not an ideal material). Best regards Reinhard Zitat von Matthew Rowles : Hi Matej You can try IMS135 - high purity alumina. https://imst/ andards.com.au%2Fproducts%2F&data=05%7C01%7Cjames.cline%40nist.gov%7C2 d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e054655c61dec%7C1 %7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJWIjoiMC4wLjAwMDAi LCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000%7C%7C%7C&sdata=r MK%2BzDuAMv2q7U6fCpu38mzuqIrTdCiQfNDPSmB%2BQZk%3D&reserved=0 It was certified against some SRM676a we already had in the lab. Matthew On Sun, 12 Nov 2023 at 22:42, Matej Dolenec wrote: Dear all, I am trying to buy NIST-676a but unfortunately unsuccessful ... I was trying to find it on NIST, ALDRICH and other sites but the standard is out of stock. Does anybody has any information if this standard will be available soon and where? If not, which standard should I use instead of NIST-676a? I was using this standard for amorphous phase identification. Regrads, Matej ++ Please do NOT attach files to the whole list Send commands to eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www/. mail-archive.com%2Frietveld_l%40ill.fr%2F&data=05%7C01%7Cjames.cline% 40nist.gov%7C2d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e0 54655c61dec%7C1%7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJW IjoiMC4wLjAwMDAiLCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000 %7C%7C%7C&sdata=nnVgkFx8mHZ%2Br%2Bng9oJ00Uz9wBy9MYDZ%2F46l%2F3%2BUGg8 %3D&reserved=0 ++ -- TU Bergakademie Freiberg Dr. R. Kleeberg Mineralogisches Labor Brennhausgasse 14 D-09596 Freiberg Tel. ++49 (0) 3731-39-3244 Fax. ++49 (0) 3731-39-3129 -- TU Bergakademie Freiberg Dr. R. Kleeberg Mineralogisches Labor Brennhausgasse 14 D-09596 Freiberg Tel. ++49 (0) 3731-39-3244 Fax. ++49 (0) 3731-39-3129 ++ Please do NOT attach files to the whole list Send commands to eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++
Re: NIST-676a
and not textured ? Le 14/11/2023 à 12:56, Reinhard Kleeberg a écrit : Hi Jim, great news, would be good to have a corundum what can be modelled with an easier profile shape model. Best regards Reinhard Zitat von "Cline, James P. Dr. (Fed)" : Hi all, SRM 676a consisted of Baikowski CR1. This material is of a non-ideal crystallite size distribution: quite broad with tales to large crystallites. SRM 676b was custom made for us by Baikowski with a more uniform crystallite size distribution in the 200 nm region. We are working on the certification, rather complex, see: doi:10.1107/S0108767311014565 . It seems that modern beamlines don't favor the large specimen size needed for our experiments. We have good data from one source, we are looking for some from another as we like to see results from more one machine. Jim James P. Cline Materials Measurement Science Division National Institute of Standards and Technology 100 Bureau Dr. stop 8370 [ B113 / Bldg 217 ] Gaithersburg, MD 20899-8523 USA james.cl...@nist.gov https://www.nist.gov/people/james-p-cline (301) 975 5793 -Original Message- From: rietveld_l-requ...@ill.fr On Behalf Of Reinhard Kleeberg Sent: Monday, November 13, 2023 1:51 AM To: rietveld_l@ill.fr Subject: Re: NIST-676a We are using Baikowski CR1 https://www.baikowski.com/en/serie/cr/ Not certified but maybe identical with SRM676a. Scale factors and cell parameters found to be within the errors. Profile shape shows similar features (also not an ideal material). Best regards Reinhard Zitat von Matthew Rowles : Hi Matej You can try IMS135 - high purity alumina. https://imst/ andards.com.au%2Fproducts%2F&data=05%7C01%7Cjames.cline%40nist.gov%7C2 d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e054655c61dec%7C1 %7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJWIjoiMC4wLjAwMDAi LCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000%7C%7C%7C&sdata=r MK%2BzDuAMv2q7U6fCpu38mzuqIrTdCiQfNDPSmB%2BQZk%3D&reserved=0 It was certified against some SRM676a we already had in the lab. Matthew On Sun, 12 Nov 2023 at 22:42, Matej Dolenec wrote: Dear all, I am trying to buy NIST-676a but unfortunately unsuccessful ... I was trying to find it on NIST, ALDRICH and other sites but the standard is out of stock. Does anybody has any information if this standard will be available soon and where? If not, which standard should I use instead of NIST-676a? I was using this standard for amorphous phase identification. Regrads, Matej ++ Please do NOT attach files to the whole list Send commands to eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www/. mail-archive.com%2Frietveld_l%40ill.fr%2F&data=05%7C01%7Cjames.cline% 40nist.gov%7C2d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e0 54655c61dec%7C1%7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJW IjoiMC4wLjAwMDAiLCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000 %7C%7C%7C&sdata=nnVgkFx8mHZ%2Br%2Bng9oJ00Uz9wBy9MYDZ%2F46l%2F3%2BUGg8 %3D&reserved=0 ++ -- TU Bergakademie Freiberg Dr. R. Kleeberg Mineralogisches Labor Brennhausgasse 14 D-09596 Freiberg Tel. ++49 (0) 3731-39-3244 Fax. ++49 (0) 3731-39-3129 ++ Please do NOT attach files to the whole list Send commands to eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++ -- -- Daniel Chateigner Professeur Normandie Universite http://www.ecole.ensicaen.fr/~chateign/danielc/ -- Editor: "Combined Analysis", Wiley-ISTE: http://eu.wiley.com/WileyCDA/WileyTitle/productCd-1848211988.html Workshops on Combined Analysis: http://www.ecole.ensicaen.fr/~chateign/formation/ -- Address: CRISMAT-ENSICAEN and IUT-Caen, Universite de Caen Normandie, campus 2 6, Bd. M. Juin 14050 Caen, France tel: 33 (0)2 31 45 26 11 daniel.chateig...@ensicaen.fr -- Open Databases: Material Properties Open Database (MPOD): mpod.cimav.edu.mx Crystallography Open Database (COD): http://www.crystallography.net/cod/ Theoretical (TCOD): http://www.crystallography.net/tcod/ Predicted (PCOD): http://www.crystallography.net/pcod/ Raman Open Database (ROD): solsa.crystallography.net/rod/ Full-Profile Search-Match (FPSM): cod.iutcaen.unicaen.fr/ -- ++ Please do NOT attach files to the who
Re:Re: NIST-676a
Dear Prof. Chateigner, I might need to update my knowledge. Do we need to consider texture effect for powder samples? Best Regards! -- Dr. Xiaodong (Tony) Wang Senior Research Infrastructure Specialist (XRD) Central Analytical Research Facility (CARF) | Queensland University of Technology Address: Level 6, P Block, Gardens Point campus, 2 George St Brisbane QLD 4000 Tel: +61 7 3138 1904 | Mob: 0452 571 680 Email: tony.w...@qut.edu.au | Web: www.qut.edu.au/ife/carf At 2023-11-14 19:58:05, "Daniel Chateigner 20210513" wrote: >and not textured ? > >Le 14/11/2023 à 12:56, Reinhard Kleeberg a écrit : >> Hi Jim, >> great news, would be good to have a corundum what can be modelled with >> an easier profile shape model. >> Best regards >> >> Reinhard >> >> Zitat von "Cline, James P. Dr. (Fed)" : >> >>> Hi all, >>> >>> SRM 676a consisted of Baikowski CR1. This material is of a non-ideal >>> crystallite size distribution: quite broad with tales to large >>> crystallites. SRM 676b was custom made for us by Baikowski with a >>> more uniform crystallite size distribution in the 200 nm region. We >>> are working on the certification, rather complex, see: >>> doi:10.1107/S0108767311014565 . It seems that modern beamlines don't >>> favor the large specimen size needed for our experiments. We have >>> good data from one source, we are looking for some from another as we >>> like to see results from more one machine. >>> >>> Jim >>> >>> >>> James P. Cline >>> Materials Measurement Science Division >>> National Institute of Standards and Technology >>> 100 Bureau Dr. stop 8370 [ B113 / Bldg 217 ] >>> Gaithersburg, MD 20899-8523USA >>> james.cl...@nist.gov >>> https://www.nist.gov/people/james-p-cline >>> >>> (301) 975 5793 >>> >>> -Original Message- >>> From: rietveld_l-requ...@ill.fr On Behalf >>> Of Reinhard Kleeberg >>> Sent: Monday, November 13, 2023 1:51 AM >>> To: rietveld_l@ill.fr >>> Subject: Re: NIST-676a >>> >>> We are using Baikowski CR1 >>> https://www.baikowski.com/en/serie/cr/ >>> >>> Not certified but maybe identical with SRM676a. Scale factors and >>> cell parameters found to be within the errors. Profile shape shows >>> similar features (also not an ideal material). >>> Best regards >>> Reinhard >>> >>> >>> Zitat von Matthew Rowles : >>> Hi Matej You can try IMS135 - high purity alumina. https://imst/ andards.com.au%2Fproducts%2F&data=05%7C01%7Cjames.cline%40nist.gov%7C2 d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e054655c61dec%7C1 %7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJWIjoiMC4wLjAwMDAi LCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000%7C%7C%7C&sdata=r MK%2BzDuAMv2q7U6fCpu38mzuqIrTdCiQfNDPSmB%2BQZk%3D&reserved=0 It was certified against some SRM676a we already had in the lab. Matthew On Sun, 12 Nov 2023 at 22:42, Matej Dolenec wrote: > Dear all, > > I am trying to buy NIST-676a but unfortunately unsuccessful ... I was > trying to find it on NIST, ALDRICH and other sites but the standard > is out of stock. Does anybody has any information if this standard > will be available soon and where? If not, which standard should I use > instead of NIST-676a? I was using this standard for amorphous phase > identification. > > Regrads, Matej > > ++ > Please do NOT attach files to the whole list > > > Send commands to eg: HELP as the subject with no > body text The Rietveld_L list archive is on > http://www/. > mail-archive.com%2Frietveld_l%40ill.fr%2F&data=05%7C01%7Cjames.cline% > 40nist.gov%7C2d945a33db074232a69808dbe414ca9a%7C2ab5d82fd8fa4797a93e0 > 54655c61dec%7C1%7C0%7C638354550207433666%7CUnknown%7CTWFpbGZsb3d8eyJW > IjoiMC4wLjAwMDAiLCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C3000 > %7C%7C%7C&sdata=nnVgkFx8mHZ%2Br%2Bng9oJ00Uz9wBy9MYDZ%2F46l%2F3%2BUGg8 > %3D&reserved=0 > ++ > > >>> >>> >>> -- >>> TU Bergakademie Freiberg >>> Dr. R. Kleeberg >>> Mineralogisches Labor >>> Brennhausgasse 14 >>> D-09596 Freiberg >>> >>> Tel. ++49 (0) 3731-39-3244 >>> Fax. ++49 (0) 3731-39-3129 >> >> >> >> ++ >> Please do NOT attach files to the whole list >> Send commands to eg: HELP as the subject with no body text >> The Rietveld_L list archive is on >> http://www.mail-archive.com/rietveld_l@ill.fr/ >> ++ >> >-- > >-- >Daniel Chateigner >Professeur Normandie Universite >http://www.ecole.ensicaen.fr/~chateign/danielc/ >-- >Editor: "Combined Analysis", Wiley-IS
