Hi Claire It sounds like you're using the Hill/Howard algorithm for quantification.
You just need to not put the details of the SiO2 phase you're using into the summation. This is equivalent to removing the ~90% attributed to the capillary, and renormalising to 100% Matthew On Tue, 14 Nov 2023 at 01:36, Claire Emily Boronski < claire.boron...@colorado.edu> wrote: > Hi All, > > > > I am trying to exclude the glass capillary from the weight percent > calculations in my Rietveld refinement. I modeled the glass capillary using > a SiO2 CIF file and made the crystallite size very small. The issue I am > having now is that in the weight percent calculation it is saying the glass > is ~90% of the weight. Does anyone know how I can exclude this phase from > the weight percent calculation? > > > > Thanks, > > Claire > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > Please do NOT attach files to the whole list <alan.he...@neutronoptics.com > > > Send commands to <lists...@ill.fr> eg: HELP as the subject with no body > text > The Rietveld_L list archive is on > http://www.mail-archive.com/rietveld_l@ill.fr/ > ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ > >
++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++ Please do NOT attach files to the whole list <alan.he...@neutronoptics.com> Send commands to <lists...@ill.fr> eg: HELP as the subject with no body text The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/ ++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++++
