Dear Rietvelders,

I have a case in measurement using conventional XRD. The case is as follow.

We have a powder consist of one phase (e.g. Al2O3). We will use conventional 
XRD. First measurement, we put 0.9 gr in the sample holder. Then we get the 
result, and call it as DATA A. Second measurement, we put 0.8 gr in the sample 
holder. Then we get the result, and call it as DATA B.

Without carrying out real measurement, and same instrumental setup is applied 
to each measurement, what can we expect about the result differences (between 
DATA A and B)? Is it true that we will get different scale factor?

Thanks for the answers.

With regards,

Budi



      

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