@lbutlr wrote:
/etc/hosts.allow:
    ALL : 185.103.253.246 : DENY

Has no effect.

I would suggest using your firewall utility to block this on tcp/ip level. If you are running Postfix under Linux the following iptables command should block this IP to accessing your smtp service on port 25:
iptables - I INPUT -s 185.103.253.246 -p tcp --dport 25 -j DROP

As someone already suggested - have a look at fail2ban.

Cheers,
Dimitar

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