These R-values are reasonable: http://xray.bmc.uu.se/gerard/supmat/rfree2000/plotter.html
On Mon, 2012-01-23 at 21:48 +0000, Sam Arnosti wrote: > Hi every one > > I have some crystals in the space group P3121. I collect 180 frames of data. > > My crystals do not diffract better than at most 2.0 angstrom, but the Rf > barely goes below 23%, > > and Rfree also remains somewhere between 28-33%. I have tried to refine my > data as much as I can. > > I do not know whether the problem is because of the bad diffraction or > collecting extra frames. > > The structure factors are also high but they get better as the crystals > diffract better. > > Thanks > > Sam -- After much deep and profound brain things inside my head, I have decided to thank you for bringing peace to our home. Julian, King of Lemurs