Dear all,
Thanks for all replies.
After water addition, R work is 0.27 and R free 0.33.
TLS and NCS results no significant approve.
Space group seem right, other space group like P21212 is worse.
>From truncate result, it is not twinning.
More detail is below:
space group P212121 a=150.099 b=148.581 c=153.429
resolution: 2.0 A
completeness: 92.3 % (58%), near complete to 2.15 A.(last shell 90.7%)
Rsym: 0.076 (34.0)
I/sigma = 20 (2.5)
Chavas Leo <[EMAIL PROTECTED]> wrote: Dear Li,
I don't know how to reduce them.
I second Tim in the fact that you should give more details on what you tried to
do as well as your statistics (resolution, data quality etc.). For instance,
did you had water molecules? Did you try TLS refinement? Do you have a wrong
symmetry?
HTH.
Kind regards.
Leo
------------------------------------------------------------
Chavas Leonard, Ph.D.
Research Associate
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Faculty of Life Sciences
The University of Manchester
The Michael Smith Building
Oxford Road
Manchester Lancashire
M13 9PT
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Tel: +44(0)161-275-1586
e-mail: [EMAIL PROTECTED]
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