I'm wondering if anybody has experience using Fullprof to refine Argonne TOF
powder diffraction data which has not been treated to account for the shape
of the incident spectrum i.e. not had incident spectrum stripped from raw
data.
Regards,
Brian Mitchell
Dr Brian J. Mitchell GRSC
IPNS Argonne
Dear All,
I am currently trying to study a sample of Ba2In2O5 (pellet form diameter =
0.9 cm. Density = 6.00 g/cm3) on GPPD at IPNS. So I am dealing with a Time
of Flight neutron powder diffraction data. I use GSAS as the refinement
package.
This is a highly absorbing sample and I understand the
I am currently analysing data taken on GPPD at IPNS on a sample of
SrFe0.8Co0.2O3-delta at 900 Celsius.
After performing a Rietveld analysis (GSAS) I can get perfectly acceptable
fits while the oxygen content is sensible for any given pO2. The Fe:Co ratio
is also as would be expected.
The proble
