Re: Sample damaging during XRD

2017-05-22 Thread Peter Y. Zavalij
rons.ornl.gov/cemd/>* > > http://www.researcherid.com/rid/B-5449-2009 > > *http://orcid.org/-0002-3447-2060 > <http://orcid.org/-0002-3447-2060>* > > ** > > > > > > *From: * on behalf of Edward Laitila < >

Re: Sample damaging during XRD

2017-05-22 Thread Payzant, E. Andrew
From: on behalf of Edward Laitila Reply-To: Edward Laitila Date: Monday, May 22, 2017 at 8:19 AM To: Shay Tirosh Cc: Rietveld list Subject: Re: Sample damaging during XRD There should be no damage but you may see a slit change in color where the beam hits the sample, a temporary change

Re: Sample damaging during XRD

2017-05-22 Thread Edward Laitila
There should be no damage but you may see a slit change in color where the beam hits the sample, a temporary change in the color center. I suggest running your generator at 45 kV and 35 mA you will get more intensity. Cheers, Ed On Sun, May 21, 2017 at 12:21 PM, Shay Tirosh wrote: > Dear Rietve

Sample damaging during XRD

2017-05-21 Thread Shay Tirosh
Dear Rietveldrs Do you know any damaging to sample that may happen during long scanning time say (3h). Specifically in case the x-ray source is Cu with Ka1+Ka2 that operates under 40mA and 40kV and the sample is metal oxides Please suggest on ref or book that elaborate on this topic. Thanks Sh