Dear Dr.Pukazhselvan,
In order to answer your question more information is needed:
Do all NaAlH4 peaks split?
Which peaks split more low angle or high angle?
Is intensities ratio of split peaks the same over whole angular range?
Peter Y. Zavalij
Director, X-ray Crystallographic Center
Departmen
Dear Mr Pukazhselvan
Since many years I am working on NaAlH4 and the dehydrogenation
products, we also have performed dozens of in situ experiments but I
have never observed a splitting of the NaAlH4 peaks. Since the system is
well understood, it sounds more like you have severe problems with y
