andrew-payzant
From: "Mibeck, Blaise"
Date: Thursday, July 25, 2019 at 4:23 PM
To: Julian Richard Tolchard , "Payzant,
Andrew"
Cc: Rietveld list
Subject: Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Been a long day. I did have a new platinum ribbon
file/e-andrew-payzant
From: Timothy Hyde
Date: Friday, July 26, 2019 at 6:07 AM
To: "Mibeck, Blaise" , Julian Richard Tolchard
, "Payzant, Andrew"
Cc: Rietveld list
Subject: RE: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Blaise,
Andrew, below correctly
-requ...@ill.fr On Behalf Of
Mibeck, Blaise
Sent: 25 July 2019 21:23
To: Julian Richard Tolchard ; Payzant, Andrew
Cc: rietveld_l@ill.fr
Subject: Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Been a long day. I did have a new platinum ribbon heater and it working well!
I
i36>
From: Julian Richard Tolchard
Sent: Thursday, July 25, 2019 10:40:26 AM
To: Payzant, Andrew ; Mibeck, Blaise
Cc: rietveld_l@ill.fr
Subject: RE: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Andrew,
I agree completely. Pt does definitely ha
Cc: rietveld_l@ill.fr
Subject: Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Jools,
You are right. “Lab grade” bottled N2 may have enough residual oxygen to cause
problems, plus it is hard to purge the chamber properly to get the pO2 low
enough to avoid issues. But an
**
From: Julian Richard Tolchard
Date: Thursday, July 25, 2019 at 10:47 AM
To: "Mibeck, Blaise" , Andrew Payzant
Cc: Rietveld list
Subject: RE: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Actually, i wouldn't recommend tha
2019 16.27
To: Payzant, Andrew
Cc: rietveld_l@ill.fr
Subject: Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
Thank you -- I will try nitrogen then!
From: Payzant, Andrew mailto:payza...@ornl.gov>>
Sent: Thursday, July 25, 2019 9:08 AM
Thank you -- I will try nitrogen then!
From: Payzant, Andrew
Sent: Thursday, July 25, 2019 9:08 AM
To: Mibeck, Blaise
Cc: rietveld_l@ill.fr
Subject: Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
STOP!!!
The tantalum foil should not
2019 at 10:03 AM
To: Rietveld list
Subject: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater
I am looking for advice on how to prepar a HTXRD sample (mounting techniques,
stage preparation, etc...). The ribbon heater is tantalum (brand new). The
sample contained ammonium di-hyd
