> But with some electronic transmission analysis no amorphous is observed.
Could the TEM investigation have led to recrystallisation?
Have you tried polarised-light microscopy to check the character of the
amorphous phase?
Cheers, Uwe
-Ursprüngliche Nachricht-
Von: rietveld_l-requ...@i
Dear Othman,
You should check if the synthesised grains in your powder are chemically
homogeneous of if they show any zonation due to growth processes. Variable
chemistry will cause broadened and/or asymmetric peaks
Are vacancies known to occur in this class of compounds? The conditions of
prepar
http://xray.uu.se/hypertext/XREmission.html
> can you remind me what the peak position of the tungsten L-alpha for the Cu
> X-ray tube?
*
Univ.-Doz. Dr. Uwe Kolitsch
Institut für Mineralogie und Kristallographie
Geozentrum, Universität Wien
Alt
gt; Armel Le Bail
> http://www.cristal.org/course/
>
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kolitsch
Institut f
their structures obviously only need to be refined.
Cheers, Uwe
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kolitsch
Institut für M
bel Becerro
> ICMSE (CSIC)
> Avda. Américo Vespucio s/n
> 41092 Sevilla (Spain)
> Tel: 34-95 4489576
> Fax: 34 95 4460665
>
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>&g
different polyhedra for identical cations then it
would be easiest to just change the type of atoms.
The inbuilt manual will help you in any other questions.
Uwe
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>&
.
Mather et al. (1995)
Mater. Chem. 5, 1177-1182
Cheers, Uwe
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kolitsch
Institut für Minera
.
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kolitsch
Institut für Mineralogie und Kristallographie
Geozentrum
Universität Wien
Althanstr. 14
A-1090 Wien
Austria
Tel +43-1-4277-53239
Fax +43-1-4277-9532
e-mail: [EMAIL PROTECTED]
home page: http://www.univie.ac.at/mineralogie/kolitsch.htm
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
In the latest edition of the ICSD there is actually the entry of
khademite you found (Bachet et al., 1981). The ICSD collection
code is 41-562.
Cheers, Uwe
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>&
)
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kolitsch
Institut für Mineralogie und Kristallographie
Geozentrum
Universität Wien
Althanstr. 14
A-1090 Wien
Austria
Tel +43-1-4277-53239
Fax +43-1-4277-9532
e-mail: [EMAIL PROTECTED]
home page: http://www.univie.ac.at/mineralogie/kolitsch.htm
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
entry = 20778
RVAL 0.026
TEST Calculated density unusual but tolerable. (Code 23)
>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
Dr. Uwe Kol
)
ITF O 1 B=0.57(4)
ITF O 2 B=0.57(4)
ITF O 3 B=0.57(4)
ITF O 4 B=0.57(4)
ITF O 5 B=0.57(4)
REM XDP (X-ray diffraction from a powder)
RVAL 0.128
>>>>>>>>>>>>>>>>>>>>>>>>>>>>&
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