Re: [sdpd] calibration problems with Silicon+gsas

2008-06-11 Thread Reinhard Kleeberg
The background looks suspicious "oscillating", not simply noisy. Maybe there are some problems with the PSD or generator stability (e.g. oscillating of cooling water temperature), or any internal or external data treatment (e.g. smoothing, interpolation..) was applied? Additionally, your profile

Re: [sdpd] calibration problems with Silicon+gsas

2008-06-11 Thread [EMAIL PROTECTED]
Hi, All: This morning i tried further refinement work and eventually i got a R value of 0.0518. As a conlusion, the critical steps are summarized: Step 1--origin selection: Thanks to the suggestion from Prof. Gottschalk, i took (1/8,1/8,1/8) origin instead of (0,0,0). It is much improved and it