Re: negative oxygen thermal parms

2005-03-07 Thread Angus P. Wilkinson
I suggest that you make sure that you are using a good absorption correction before looking at more exotic causes for your negative thermal parameters. Angus At 03:46 PM 3/7/2005 +, you wrote: Natale Perchiazzi wrote: I am presently refining a structur

lanthanum sulfate

2005-03-07 Thread Gerard, Garcia S
Dear all,   Does anybody know where can i get a powder XRD pattern of lanthanum sulfate from? I can't find it in the CDS and i'm getting nuts 'cos i just could find a rough draw in a paper.   Thanks.   gerard  

Re: negative oxygen thermal parms

2005-03-07 Thread Jacco van de Streek
Natale Perchiazzi wrote: I am presently refining a structure of a REE-Na silicate. The data were collected in capillary geometry, CuKa1 radiation, long (50secs) counting times and a step of 0.02, up to 100° 2theta. After some refinement cycles, I get reasonable positional and displacement parame

negative oxygen thermal parms

2005-03-07 Thread Natale Perchiazzi
Dear All, I am presently refining a structure of a REE-Na silicate. The data were collected in capillary geometry, CuKa1 radiation, long (50secs) counting times and a step of 0.02, up to 100° 2theta. After some refinement cycles, I get reasonable positional and displacement parameters for al