And here some more small molecule crystallization links.
http://xray.chem.ufl.edu/growing%20tips.htm
http://mic.ucla.edu/x-ray%20diffraction/tutorials_crystalgrowing.htm
http://www.nottingham.ac.uk/~pczajb2/growcrys.htm
Jose Antonio Cuesta-Seijo
On Jul 18, 2007, at 5:56 PM, Green, Todd wrote:
Hello Todd.
An experienced synthetic chemist is your best source of help here,
but otherwise have a look at these links.
And greasy molecules are no problem. Organic chemists crystalize them
like candy!
http://www.xray.ncsu.edu/GrowXtal.html
http://web.mit.edu/x-ray/cystallize.html
http://64
Anthony had given some good advice.
In addition, Any organic solvent may be helpful. We often use methanol and
chloroform.
= 2007-7-19 6:12, your message: Re: [ccp4bb] advice for
crystallizing hydrophobic small molecules=
Hi Todd
I have worked in the past
Hi Todd
I have worked in the past with crystallization of dozens of small
molecules, several of them steroids which are hydrophobic. What I did
was, first get the small molecule into the solution. The solvent can
be dimethyl formamide, dimethyl sulfoxide, chloroform or anything
that I ca