Hi all,
Thank you all how have replied for their kind suggestions and diagnosis of
collected data.
sincerely
Debajyoti
On Sat, 26 Mar 2011 04:44:42 +0530 wrote
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Hi all,
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I have collected one iodine soaked data in our home source, and processing the
data using HKL2000. Exposure tim
The most likely explanation is that you have a cracked crystal or your
crystal has split from radiation damage around the frame 70.
If you had a cracked crystal from the start, the spot overlap between
crystals would change when the sample was rotated. In such cases, it may
happen that the program
Hi all,
I have collected one iodine soaked data in our home source, and processing the
data using HKL2000. Exposure time per frame is 5min/1 degree.
While processing I have noticed that the Chisq values, cell parameters and
rotation change Vs frame are deviating like anything. Please find the p
