Dear CCP4bb members,
I am new to iMosflm data processing (I use HKL2000 but I really want to
learn iMosflm). After automatic index, cell refinement and integration in
iMosflm, I got 2 warnings.
1. Error in detector gain. BGRATIO of my data lies outside the 0.7 to 1.3
range (mine is 0.64) Imosfl
I had some cases, when path INTEGRATE.HKL -> Aimless gave data, from
which it was not possible to solve structure by Phaser. It looked like
structure solved, but then I got 45-50% Rwork/free. There were no
problems with XDS_ASCCI.HKL -> Aimless (Not scale, just merge) path.
Jan
On 11/24/2016 0
Dear Napo,
I imagine this article, although rather wide ranging in its content, will
be of assistance:-
http://journals.iucr.org/d/issues/2005/06/00/ic5050/
More generally you might consult Chayen, Helliwell and Snell
"Macromolecular Crystallisation and Crystal Perfection" Published by OUP
and IUCr
Dear David,
The following will be of interest:-
*J. Chem. Soc., Faraday Trans.*, 1993, *89*, 2667-2675 (*DOI:
*10.1039/FT9938902667
)
and
Y P Nieh PhD Thesis 1997 available at :- http://ethos.bl.uk/Home.do
[ie just search on his name and the pdf is available.]
All best wishes,
John
On Fri, Dec 2
