I tried it, and I first I was getting the same result as you...
Choosing to boot the USB key, result in message to insert a valid disk...

Until I realized that I had written a .iso file on the USB key rather than the 
freshly dowloaded .img file.
(More precisely was wrongly writing FD13LIVE.iso file).

What works for me is:
https://www.ibiblio.org/pub/micro/pc-stuff/freedos/files/distributions/1.3/official/FD13-LiteUSB.zip
more precisely the FD13LITE.img file.

Then the boot order is important... Might consider to try to boot a Linux ISO 
in Legacy mode to be sure
you get the boot order right.



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