Far as I understand, twins may or may not have macroscopically
recognizable features. Macroscopic (and microscopic) features like
face angles, reaction on etching, polarization of light, etc. can
sometimes indicate twinning for at least a subset of cases, e.g. in
diamond, some forms of quartz, etc. (see Hahn and Klapper, "Twinning of
Crystals" in the International Tables for Crystallography).

Best wishes,
Navdeep

https://scholar.google.de/citations?user=ZqU1AE0AAAAJ


---
On 17.03.21 11:12, Ana Luísa Moreira de Carvalho wrote:
> Just a short note on this: I often see colleagues using the word
> “twinning" when referring to a crystal that is actually multiple (not
> single).
> 
> I think much confusion arises from this. For me, a twin crystal is the
> one that looks single under the microscope and only intensity statistics
> reveal that the diffraction comes from more than one crystal.
> 
> If a crystal looks multiple, i do not call it a twin. Am i being too
> meticulous on this?
> Thanks!
> 
>> On 16 Mar 2021, at 13:31, Eleanor Dodson
>> <[email protected]
>> <mailto:[email protected]>> wrote:
>>
>> You usually detect twinning most reliably from the intensity
>> statistics - CCP4I2 and Xtriage report those..
>> Eleanor
>>
>> On Tue, 16 Mar 2021 at 07:31, Marina Gárdonyi
>> <[email protected]
>> <mailto:[email protected]>> wrote:
>>
>>     Dear all,
>>
>>     thanks to all who helped me solving the question. You sent me a
>>     lot of 
>>     comments and information I have not taken into account.
>>     After reading all the answers, I have come to the conclusion that
>>     the 
>>     spots that are very close to each other come from the long cell axis 
>>     (57-57-160) and that twinning can probably not be seen in my case. I 
>>     should have mentioned that the diffraction images came from an 
>>     in-house x-ray machine, recorded with a 0.5 degree rotation range.
>>
>>     Thank you all again!
>>
>>     Kind regards,
>>     Marina
>>
>>     -- 
>>     Marina Gárdonyi
>>
>>     PhD Student, Research Group Professor Dr. Klebe
>>
>>     Department of Pharmaceutical Chemistry
>>
>>     Philipps-University Marburg
>>
>>     Marbacher Weg 6, 35032 Marburg, Germany
>>
>>     Phone: +49 6421 28 21392
>>
>>     E-Mail: [email protected]
>>     <mailto:[email protected]>
>>
>>     http://www.agklebe.de/ <http://www.agklebe.de/>
>>
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