Interesting observation. In our home X-ray lab, we constructed a liquid 
nitrogen dumping station from a large garbage can filled with sand to about 12 
inches. To keep the sand out of the dewars we topped the sand with a large wad 
of screen-door netting. All items can easily be purchased from a local home 
improvement store, and the screen-door netting is super cheap (plus it makes it 
easy to remove the stray bits of garbage that mistakenly find their way into 
the nitrogen dump/garbage can (you can put a sign that states, “not for 
garbage” on a garbage can, but you can’t get 100% compliance, LOL).

Diana

**************************************************
Diana R. Tomchick
Professor
Departments of Biophysics and Biochemistry
UT Southwestern Medical Center
5323 Harry Hines Blvd.
Rm. ND10.214A
Dallas, TX 75390-8816
diana.tomch...@utsouthwestern.edu<mailto:diana.tomch...@utsouthwestern.edu>
(214) 645-6383 (phone)
(214) 645-6353 (fax)




On Dec 4, 2020, at 10:42 AM, Nukri Sanishvili 
<sannu...@gmail.com<mailto:sannu...@gmail.com>> wrote:


EXTERNAL MAIL

Hi John,
I think I know what might have happened:
Many of the MX beamlines at the APS use some sort of filler in the containers 
where the LN2 is dumped. If I remember correctly, one of the beamlines is using 
fine gravel for this purpose. Also, it is required that before shipping, the 
dewars are emptied - i.e. don't contain liquid. Now, imagine somebody dumping 
the liquid into the grave-filled container without removing the blue cap and 
without holding the dewar in the air - i.e. the top of the dewar with the cap 
on is slightly buried into the gravel. Upon straightening the dewar up, the 
blue cap would scoop up a little bit of the gravel. Distribution of the pebbles 
on your picture is also noteworthy. It suggests the side where the pebbles are 
was the side dipped into the gravel.
You might want to discuss this with your beamline host.
Best,
Nukri

On Fri, Dec 4, 2020 at 10:05 AM Tanner, John J. 
<tanne...@missouri.edu<mailto:tanne...@missouri.edu>> wrote:
When we opened our CX100 shipping dewar returned from APS via FedEx this week, 
we observed what appears to be tiny rocks on the rim below the foam neck core:

https://www.dropbox.com/s/ky09a1vbm9t0mrl/CX100withrocks.png?dl=0

Has anyone seen this before? Is this perhaps the absorbent material from the 
inside of the dewar?

Thanks,

Jack

John J. Tanner
Professor of Biochemistry and Chemistry
Associate Chair of Biochemistry
Department of Biochemistry
University of Missouri
117 Schweitzer Hall
503 S College Avenue
Columbia, MO 65211
Phone: 573-884-1280
Email: tanne...@missouri.edu<mailto:tanne...@missouri.edu>
https://cafnrfaculty.missouri.edu/tannerlab/
Lab: Schlundt Annex rooms 3,6,9, 203B, 203C
Office: Schlundt Annex 203A

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