I have noticed it with new pucks (most likely some kind  of grease from 
manufacturing) and later on when used in dry shipping dewars that has old 
absorbent coating. Also it might be that your dewar is not holding vacuum very 
well. Usually it can be cleaned with compressed air but have decided to change 
dewar anyway and problem disappeared.


Michal

On Feb 21, 2020, at 18:40, Diana Tomchick <diana.tomch...@utsouthwestern.edu> 
wrote:


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I believe my technician decided that it was due to the breakdown of the 
adsorbent foam in our oldish shipping dewar, as it stopped happening once we 
replaced that particular dewar.

But I would be open to other explanations.

Diana

**************************************************
Diana R. Tomchick
Professor
Departments of Biophysics and Biochemistry
UT Southwestern Medical Center
5323 Harry Hines Blvd.
Rm. ND10.214A
Dallas, TX 75390-8816
diana.tomch...@utsouthwestern.edu<mailto:diana.tomch...@utsouthwestern.edu>
(214) 645-6383 (phone)
(214) 645-6353 (fax)

On Feb 21, 2020, at 6:33 PM, Emilia C. Arturo (Emily) 
<ecgart...@gmail.com<mailto:ecgart...@gmail.com>> wrote:


EXTERNAL MAIL

Hi All,

We have been noticing lately that our crystal pucks return from different 
beamlines coated with the same powdery material. For the record, we typically 
undo our pucks, clean the assemblies and dry out the pucks within a day of 
receiving the shipping dewar, but notice the same thing regardless of how long 
between receiving the dewar and disassembling the pucks. Have any of you 
experienced this sort of thing, or have suggestions of what might be the cause 
and/or the powdery material?

Regards,
Emily.

--
"Study as if you were going to live forever; live as if you were going to die 
tomorrow." - Maria Mitchell

"I'm not afraid of storms for I'm learning to sail my ship."  - Louisa May 
Alcott


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