Dear Rohit, Try to run sfcheck or XTRIAGE and check, if your data is fine. Check for twinning or pseudo-translation. You can send your processed mtz to me and I would be more than happy to help you.
You can look into cumulative intensity distribution (if you processed with XDS, it will be in CORRECT.LP file) and it will give you indication of twinning. Thank you Rajesh ---xxxxx---- With regards Rajesh K. Harijan, Ph.D. Albert Einstein College of Medicine 1300 Morris Park Ave., Bronx, NY 10461 Tel: 718.430.2777 | Fax: 718.430.8565 On Wed, Dec 14, 2016 at 10:02 AM, rohit kumar <rohit...@gmail.com> wrote: > Dear All, > > I am solving a data of 2.5 A (C121 space group). Right now the R/Rfree > values are 26/33, after many cycles of refinements (With or With out water) > the R/Rfree values still same. Zanuda suggests that the space group seems > to be correct and the model is looking fine in coot. > Some one suggest what is the main problem. > Should I again process my data? And what is the best way to fine right > space group (If problem with space group). > Please tell me if you need any information regarding may data. > > -- > WITH REGARDS > Rohit Kumar Singh > Lab. no. 430, > P.I. Dr. S. Gourinath, > School of Life Sciences, > Jawaharlal Nehru University > New Delhi -110067 >