Further to what Nat wrote which I completely agree with, you should tell us the 
following:

1. Expecting signal of a Calcium atom and expected signal of a Magnesium atom.

2. Are there any intrinsic anomalous scatterers in the structure that you trust 
such as sulfurs from methionines and cysteines or even selenium at 
selenomethionines?  What are their expected signals and do you see those 
signals?  If not, why not?  Basically, these should give one a positive control 
which they can check their experiment with.

________________________________
From: CCP4 bulletin board [CCP4BB@JISCMAIL.AC.UK] on behalf of Faisal Tarique 
[faisaltari...@gmail.com]
Sent: Monday, April 21, 2014 5:36 PM
To: CCP4BB@JISCMAIL.AC.UK
Subject: [ccp4bb] anomalous signal for Mg and Calcium

Dear all

Just in the continuation ...

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