Rex Palmer wrote:
What seems to be a possible sulphate has been identified in our electron
density.
What steps could/should be taken to confirm or consolidate this assignment that
would satisfy referees?
Rex Palmer
Birkbeck College
If you place a sulphate and it refines in a sensible way - temperature
factors for the group more or less agreeing that is good.
Is there a decent set of H bonds?
Was there sulphate available in the medium?
is there a anom peak marking the S position - but you need good data to
hope to find this - you can verify quality by checking all other S in
the crystal
Eleanor
