Dear Xianchidong
If you are sure it is a divalent ion, Mg would be hard to detect even at
a wavelength of 2.07A.
best
Preben

xianchidong wrote:
> Dear All:
> When I solved the crystal structure of protein, I found a metal
> binding in it. But however, I can not decide which type of atom it is.
> I tried ICP-AES and the result suggested the protein contained Ca. I
> tried to get anomalous signal at the wavelength of 2.07A. And I
> collected the 360 degree with the spacegroup P6 and the average
> redundancy is 19.6. But still I can not see the anomalous signal for
> that metal even I can see clearly the anomalous signal for sulfur.
> Does anybody have suggestions for me?
> Thanks in advance.
> 2009-06-30
> ------------------------------------------------------------------------
> xianchidong


-- 
Jens Preben Morth, Ph.D
Aarhus University
Department of Molecular Biology
Gustav Wieds Vej 10 C
DK - 8000 Aarhus C
Tel. +45 8942 5257, Fax. +45 8612 3178
j...@mb.au.dk
website: http://person.au.dk/da/j...@mb

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