Dear All

sorry for a non-ccp4 related question. 

what is the typical concentration of detergents used in membrane protein 
purification? 
Is it usually within 1-10 times of CMC? 

My collaborator was using 10% DDM in purifying a membrane protein. I suggested
to reduce it and now he is working with 2% DDM. He said lower than that the 
protein 
is not soluble. 

so another question is, can we purify the membrane protein first at high 
concentration
of one detergent (say, 2% DDM), and then screen different detergents later to 
find a 
better one? Or it is better to screen the detergents first before purification? 
 

any suggestions will be appreciated. 

Have a nice holiday!

Rongjin Guan 

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